mar249 - Advanced NMR Spectroscopy

mar249 - Advanced NMR Spectroscopy

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Module label Advanced NMR Spectroscopy
Modulkürzel mar249
Credit points 6.0 KP
Workload 180 h
Institute directory Institute for Chemistry and Biology of the Marine Environment
Verwendbarkeit des Moduls
  • Master's Programme Marine Environmental Sciences (Master) > Mastermodule
Zuständige Personen
  • Vemulapalli, Sahithya Phani Babu (module responsibility)
Prerequisites
Keine
Skills to be acquired in this module

Participants who successfully complete this course covering the topics mentioned will greatly benefit from a comprehensive understanding of nuclear magnetic resonance (NMR) spectroscopy and its applications. They will gain proficiency in utilizing the product operator formalism to describe 2D NMR experiments such as COSY, TOCSY, HSQC, HMBC, NOESY/ROESY, and more. This knowledge will enable them to analyze complex mixtures, perform structural analysis, and explore advanced NMR techniques like J-RES, DOSY, non-uniform sampling, and pure-shift NMR. Students will also learn about selective excitation, quantitative NMR, and the fundamentals of solid-state NMR. Moreover, they will explore the practical applications of NMR spectroscopy in various fields, including Environmental Science, Chemistry, and Biology. In particular, the course will focus on the structural analysis of marine DOM (dissolved organic matter) through NMR, providing hands-on experience with data acquisition, processing, and interpretation. Overall, completion of this course will equip participants with a strong foundation in NMR spectroscopy and its diverse applications, empowering them to excel in research, industry, or further studies in related fields.

The hands-on NMR training will take place on the state-of-the-art Bruker Avance Neo 800 MHz NMR instrument, which is equipped with a variety of helium-cooled cryoprobes.

Module contents

Product operator formalism for the description of 2D NMR experiments, COSY, TOCSY, HSQC, HMBC, NOESY/ROESY, Complex mixture analysis, J-RES, DOSY, Advanced NMR methods, Non-uniform sampling, NMR supersequences, Pure-shift NMR, Selective excitation, Quantitative NMR, Fundamentals of solid-state NMR, Applications of NMR spectroscopy in Environmental Science, Chemistry and Biology, Structural analysis of marine DOM by NMR, Hands-on NMR spectroscopy for the structural analysis of marine DOM and model organic mixtures, NMR data acquisition, processing and interpretation.

Literaturempfehlungen

Die Teilnehmenden erhalten ein Vorlesungsskript. Auf weitere Literatur wird in der Veranstaltung hingewiesen.

Links
Language of instruction English
Duration (semesters) 1 Semester
Module frequency jährlich
Module capacity 8
Form of instruction Comment SWS Frequency Workload of compulsory attendance
Lecture 2 SoSe 28
Exercises 4 SoSe 56
Präsenzzeit Modul insgesamt 84 h
Examination Prüfungszeiten Type of examination
Final exam of module

Klausur am Ende der Veranstaltungszeit oder

fachpraktische Übung oder mündliche Prüfung nach Maßgabe der Dozentin oder des Dozenten.

1 benotete Prüfungsleistung

Klausur oder mündliche Prüfung oder fachpraktische Übung

 

Aktive Teilnahme
Protokollierung der jeweils durchgeführten Versuche bzw. der praktischen Arbeiten, Diskussion von Seminarbeiträgen oder Darstellungen von Aufgaben bzw. Inhalten in der Lehrveranstaltung in Form von Kurzberichten oder Kurzreferat. Die Festlegung hierzu erfolgt mit dem Lehrenden zu Beginn des Semesters bzw. zu Beginn der Veranstaltung.

Abgabe eines Praktikumsberichtes


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